Topic
: Scanning
Electron / Ion / Probe
Microscopy in Materials
Characterization(SEIPM)
Concepts Covered
ØLens aberrations
ØHistory on electron microscope
ØLight versus electron
ØWhat is a scanning electron microscope (SEM)?
Early History of Electron Microscope •1931
-
The
German
physicist
Ernst Ruska and
the
electrical
engineer
Max Knoll constructed
the
first transmission electron microscope
(TEM).
•1935
-
Knoll built a
first
“scanning
microscope”
The
resolution
limit
was
~100
mm. •1937/1938 - Manfred
von Ardenne pioneered
the
scanning
electron
microscope
by
adding
scan
coils
to
a transmission electron microscope. It
is
actually
a
STEM. •1938
-
Ruska and Bodo von Borries improved
the
resolution
of
TEM
to
10
nm. •1938
-
The
first
practical
electron
microscope
was
constructed
at
the
University
of
Toronto,
by
Eli Franklin Burton and
students
Cecil
Hall,
James
Hillier,
and
Albert
Prebus •1939
-
Siemens
produced
the
first commercial
TEM •1942
–
The
first
true
SEM
was
developed
by
Vladimir Zworykin,
who
showed
topographic
contrast using secondary
electrons. •1952
–
Oatley and McMullan achieved
a
resolution
of
50
nm
using
the
SEM
built by
them. •1960
–
Everhart and Thornley improved
secondary
electron
detection. •1963
–
Pease and Nixon combined
previous
improvements
in
one SE M
with
three
magnetic
lenses and a E-T detector
•1965
–
The
first commercial
SEM, the Cambridge
Scientific
Instruments
Mark
I “Stereoscan”
Light versus Electron
•Wavelength •Scattering
•Charge •Type of lens can be used
1. Wavelength of electron in an electron microscope
2. What is a SEM?
The S E M is an instrument that scans a
sample
surface
with
a
finely
converged
electron
beam under vacuum,
detects
the
information
(signals)
produced
at
that
time
from
the
sample,
and presents an enlarged
image
of
the
sample
surface
on
the
monitor
screen.
Conclusions
ØElectron can have small wavelength – thus can produce higher
resolution image
ØDue to its charge, we can use electromagnetic lenses
in microscope
ØLens
aberrations reduce the performance of a microscope
References
ØElectron Microscopy and Analysis by Goodhew and Humphreys, 1988, Taylor & Francis
ØScanning Electron Microscopy and X-ray Microanalysis by Joseph Goldstein et al., 3rd edition, 2003, Springer
Science +
Business Media
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